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MSE 690 Oct 04 2019, 3:30 pm, Vilmali Lopez-Mejias
by Ku Blanco, Aury Y 04 Oct '19

04 Oct '19

Good Morning all, Our guest, Dr. Lopez-Mejias is in the building and is looking forward to seeing you all at the seminar presentation this afternoon! Forwarded on behalf of Prof. Carlos Martinez: [cid:image002.jpg@01D57A9D.6E37EA30] Thank you, Aury Ku Administrative Assistant Purdue University School of Materials Engineering Neil Armstrong Hall of Engineering 765/494-4100 akublanc(a)purdue.edu<mailto:staceyl@purdue.edu> [https://www.purdue.edu/brand/images/Purdue_University-150_Years_of_Giant_Le…]

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Seminar Notice for Nicholas Richter Oct. 10, at 8:30 a.m., in ARMS 3109. " Micropillar Compression Studies of Deformation Behavior in Nanostructured FCC Metals"
by Son, Rosemary E 03 Oct '19

03 Oct '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Micropillar Compression Studies of Deformation Behavior in Nanostructured FCC Metals" By Nicholas A. Richter Purdue MSE Preliminary Exam Advisor: Professor Xinghang Zhang ABSTRACT Nanostructured metals have peaked significant interest for automotive and aerospace applications as they can drastically improve a metal's mechanical properties. These structures, including nanocrystalline and nanotwinned metals, can lead to novel deformation behaviors and a significant improvement of mechanical properties. As both devices (nanowires, NEMS) and microstructural features approach the nanoscale, there is an opportunity to elucidate the mechanisms governing deformation in these systems. Micropillar compression provides an avenue to explore their mechanical behavior. New insight to deformation in nanostructured metals can be gained through in-situ videos of micropillar compression in the SEM, as well as post-compression microstructural analysis using TEM. This review focuses on microcompression of nanostructured face centered cubic (FCC) metals due to the abundance of literature on these systems. It also details possible challenges faced with designing micropillar compression experiments and postcompression analysis. Keywords: Micropillar compression, Size effects, Nanostructured Metals, FCC metals, Micromechanical Testing Date: Thurday, October 10, 2019 Time: 8:30 A.M. Place: ARMS 3109

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Seminar Reminder for Tianyi Sun's Preliminary Exam. Seminar, Monday, October 7, at 8:30 a.m., in ARMS 3115. " Irradiation Induced Microstructural Evolutions in FeCrAl Alloys"
by Son, Rosemary E 03 Oct '19

03 Oct '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Irradiation Induced Microstructural Evolutions in FeCrAl Alloys" By Tianyi Sun Purdue MSE Preliminary Exam Advisor: Professor Xinghang Zhang ABSTRACT Development of advanced nuclear reactors poses significant challenges for structural materials that need to operate under high temperatures, higher pressure, higher irradiation dose, and often corrosive environments. FeCrAl alloy, one class of ferritic steel with high Cr and Al content, is deemed as one of the most promising candidates for accident tolerant applications. Two orders of magnitude lower steam oxidation rate at high temperature (< 1500 °C) than currently used Zirconium based alloys in commercial light water reactors gives FeCrAl alloys a clear edge over many other candidates under accident scenarios. However, long time exposure to radiation generates defect clusters and causes phase separation in FeCrAl alloys accompanied by degradation of mechanical properties, such as radiation-induced hardening and embrittlement. This report examines recent studies on microstructural evolutions in irradiated FeCrAl alloys and point out some future studies that are needed to better understand the mechanisms of radiation damage in FeCrAl alloys and further improve their radiation tolerance. Keywords: FeCrAl alloys, high temperature oxidation, dislocation loop formation, α' phase separation, irradiation hardening Date: Monday, October 7, 2019 Time: 8:30 A.M. Place: ARMS 3115

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Seminar Reminder for Raheleh M. Rahimi's PhD Final Exam. Seminar, Friday Oct 4, at 1:30 p.m., in HAMP 2118. Exam same day, at 2:30 in ARMS 2007. " Micromechanical Analysis and Characterization of Materials with Spatially Distinct Microstructural Featur
by Son, Rosemary E 03 Oct '19

03 Oct '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Micromechanical Analysis and Characterization of Materials with Spatially Distinct Microstructural Features" By Raheleh Mohammad Rahimi Purdue MSE Ph.D. Final Exam Advisor: Professor David F. Bahr ABSTRACT Correlations between materials microstructural properties and mechanical behavior are important for materials development. As materials characterization methods have been restricted to instrument accessibility, sample dimensions and economical aspects, developing functional techniques in order to obtain better understanding of materials behavior in micro and nano scale is crucial. Procedures for assessing and interpreting the mechanical responses at small scales, combined with investigating the microstructure are considered as significant steps to design and develop the effective frameworks for evaluating bulk properties. This research demonstrates that how fundamental understanding of microstructures can assist interpreting of mechanical performance of bulk materials. Testing of materials at small scales is very important because the mechanical failure of any bulk material starts with the formation, extension, or local accumulation of initially small defects, leading finally to a fracture. Thus, any bulk material profits from an in-depth understanding of its deformation and mechanical phenomena at the nano- and micrometer length scale. This thesis shows how the micro constituents' interactions and grain boundaries reactions to dislocations in alloys and thin films contribute to understanding material flow behavior and differences in the mechanical properties of these materials in a wide range of material systems with variations in appropriate sizes which need to be probed. Among other things, this work shows that sources of variation can be specified and quantified as predictive tools for designing materials. The strength and strain hardening of martensite and ferrite in a dual phase steel with a grain size less than 5 μm were determined using an inverse technique. The yield strengths of the ferrite and martensite phases are calculated as 370 MPa and 950 MPa respectively. The calculated hardening exponent of the alloy was exactly same as tensile test result (0.11). The constrain phenomena was obviously effective in deformation of this elastic-plastic alloy. Also the differences in hardness and pop-in behavior were used to understand of the influences of different types of grain boundaries, high density dislocations, and twins in Al thin films before and after plasticity. Date: Friday, October 4, 2019 Time: 1:30 P.M. Place: HAMP 2118

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MSE 690 Oct 10 2019 Jinkyoung Yoo - Faculty Meetings
by Ku Blanco, Aury Y 01 Oct '19

01 Oct '19

Hi all, Once more I am reaching out seeking interested participants in meeting with an upcoming guest. I invite you to review the notice below and check your calendars for this day! We will be setting up meetings on Thursday, October 10th from 9:30-11:30 am and again from about 2-4 pm. Please let me know if you or any of your students are interested in a time. [cid:image002.png@01D57864.3E0E87A0] Thank you, Aury Ku Administrative Assistant Purdue University School of Materials Engineering Neil Armstrong Hall of Engineering 765/494-4100 akublanc(a)purdue.edu<mailto:staceyl@purdue.edu> [https://www.purdue.edu/brand/images/Purdue_University-150_Years_of_Giant_Le…]

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MSE Safety & Equipment Newsletter for September/October 2019
by Erk, Kendra A 30 Sep '19

30 Sep '19

PDF of newsletter available here: https://engineering.purdue.edu/Intranet/Groups/Schools/MSE/Facilities/Safet… MSE Safety & Equipment Newsletter for September/October 2019 **** Important upcoming dates **** * Wednesday, October 2nd - "Refresher" safety training seminar at 3:30 PM in ARMS 1010 (during MSE 390). Please bring your smart phone if you plan to attend. * Friday, October 18th - Deadline for ARMS lab supervisors to submit their building inspection abatement reports to Jenni Fifer. **** MSE Lab Safety Blackboard course updates **** * Safety training FAQ * Documents related to HF training and use Reminder: To self-enroll in this Blackboard course, click here<https://mycourses.purdue.edu/webapps/blackboard/execute/viewCatalog?id=&typ…> . **** Annual ARMS building inspection **** REM completed their annual fall inspection of the Armstrong lab spaces on behalf of OSHA in early September. A hard-copy list of issues that must be abated/corrected was distributed to lab supervisors (red folders in your ARMS mailbox). Please correct the issues associated with your lab space and return the form to Jenni Fifer (ARMS 2207) by October 18th. **** HF reminder **** All activities involving the use of any quantity of hydrofluoric acid ("HF") should ONLY occur within the fume hood in ARMS 2132 (the polishing lab) and are not allowed to take place in any other lab spaces within ARMS or MSEE. HF activities should ONLY be performed by individuals who have received training by the MSE Safety Officer. Contact Jenni Fifer<mailto:fiferj@purdue.edu> for questions or to request training. **** Lab access reminders**** Please read the instructions on MSE Lab Safety Blackboard course and the lab access request before filling one out. This will save time and prevent delays in receiving lab access. If you have any questions or concerns about lab access, feel free to stop by ARMS 2207 to speak with the MSE Safety Officer (Jenni Fifer<mailto:fiferj@purdue.edu>). Helpful lab access request form reminders are below: * If you have had lab access in ARMS or MSEE at any point in the past, DO NOT mark "New User" in the lab access form. * Submit your forms by Thursday afternoon to receive lab access Friday. If you submit a form on Friday, you will not receive access until the following Friday. * Make sure to include billing information if requesting access to a key fee lab. * Make sure to CC mse-safety(a)purdue.edu<mailto:mse-safety@purdue.edu> on emails requesting faculty permissions. **** Notice on VC-50 slow-speed saws in ARMS 2136 **** Please be sure to follow new procedures outlined near the VC-50 saws in ARMS 2136. These include: * For harder materials (tool steel, carbides, ceramics), use the saw with the equipped diamond cutting wheel. * For softer materials (most metals), use the saw equipped with the aluminum oxide cutting wheel. * Do not use the diamond cutting wheel to cut epoxy or bakelite mounting media (use the aluminum oxide wheel instead). **** New automatic mounting presses **** The MSE Equipment Committee is considering purchasing/replacing automated mounting presses in ARMS 2136. We are seeking your feedback on mounting sizes. Please fill out the following Qualtrics to get your voice heard! https://purdue.ca1.qualtrics.com/jfe/form/SV_b88loyXvz1dr1jv **** Equipment reporting reminder **** If you encounter a piece of broken equipment, or have any questions about a specific piece of equipment, you should contact a member of the MSE Technical Staff: * For general equipment: Tim VanMeter<mailto:tcvanmet@purdue.edu>, Darren Pauly<mailto:dpauly@purdue.edu> * For mechanical testing equipment: Jenni Fifer<mailto:fiferj@purdue.edu> * For analytical (iLab) equipment: Talukder Alam<mailto:alam18@purdue.edu> **** Annual "refresher" trainings **** As described in the MSE safety training policy (emailed on Sept. 6 and posted here<https://engineering.purdue.edu/Intranet/Groups/Schools/MSE/Facilities/Safet…>), each academic year, all faculty, technical staff, undergraduate students, graduate students, postdoctoral researchers, and other research-active personnel are required to attend one in-person safety "refresher" training. Options for this refresher training include safety seminars led by the MSE Safety Officer as well as research-specific safety meetings led by an MSE Faculty member. The latter meeting must address a short series of Powerpoint slides provided by Prof. Erk which include guidance on how to document the training within MSE records. **** Important links and contact information **** * For general safety questions, concerns, and lab access issues: mse-safety(a)purdue.edu<mailto:mse-safety@purdue.edu> or speak directly to MSE Safety Officer Jenni Fifer<mailto:fiferj@purdue.edu> (ARMS 2207) * For iLab equipment training and issues: Talukder Alam<mailto:alam18@purdue.edu> (ARMS 2207) * Equipment/Safety/Consumables Reporting Form<https://purdue.ca1.qualtrics.com/jfe/form/SV_7QcGyO9IVMwWRPD?_ga=2.24554381…> * Purdue REM Researcher's Guide<https://www.purdue.edu/ehps/rem/laboratory/researchers.html#cs2> (all new researchers should check this out...) * ARMS general safety information<https://engineering.purdue.edu/Intranet/Groups/Facilities/ArmstrongHall> Thanks for reading everyone and have a GREAT October! Prof. Erk and the MSE Safety Committee

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FW: Concerns about VC-50 saw use in ARMS 2136
by Stacey, Lisa A 24 Sep '19

24 Sep '19

Forwarding on behalf of Darren Pauly: All, In ARMS 2136, we have two Leco VC-50 saws set up for use. One saw is equipped with a diamond cutting wheel; this is meant for cutting harder materials. The other saw is dedicated for the cutting of softer materials; it is equipped with an aluminum oxide cutting wheel. Each saw is marked appropriately. In addition, there is a chart (taken out of the user's manual) posted between the two saws indicating the appropriate cutting wheel to use. I am sending this email to clarify an issue that has surfaced recently. I have noticed that some students have been using the diamond cutting wheel to cut epoxy sample mounts and bakelite sample mounts. To be fair, these materials are not listed on the chart that is in-between the machines. I asked a student to research the hardness characteristics of these epoxy sample holders and according to his research, both of the sample mounts are considered softer materials and must be cut with the aluminum oxide cutting wheel. Please DO NOT use the diamond cutting wheel to cut these sample mounts; doing so will lead to premature failure of the diamond cutting wheel. I will be getting the appropriate notices related to this posted in ARMS 2136 shortly. If you would like some more information about this issue, please feel free to stop by my office (ARMS 2200-1) for assistance. Thank you for your cooperation. Regards, Darren Darren Pauly Laboratory Technician VIII School of Materials Engineering Purdue University (765) 494-7703

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Seminar Notice for Tianyi Sun's Preliminary Exam. Seminar, Monday, October 7, at 8:30 a.m., in ARMS 3115. " Irradiation Induced Microstructural Evolutions in FeCrAl Alloys"
by Son, Rosemary E 23 Sep '19

23 Sep '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Irradiation Induced Microstructural Evolutions in FeCrAl Alloys" By Tianyi Sun Purdue MSE Preliminary Exam Advisor: Professor Xinghang Zhang ABSTRACT Development of advanced nuclear reactors poses significant challenges for structural materials that need to operate under high temperatures, higher pressure, higher irradiation dose, and often corrosive environments. FeCrAl alloy, one class of ferritic steel with high Cr and Al content, is deemed as one of the most promising candidates for accident tolerant applications. Two orders of magnitude lower steam oxidation rate at high temperature (< 1500 °C) than currently used Zirconium based alloys in commercial light water reactors gives FeCrAl alloys a clear edge over many other candidates under accident scenarios. However, long time exposure to radiation generates defect clusters and causes phase separation in FeCrAl alloys accompanied by degradation of mechanical properties, such as radiation-induced hardening and embrittlement. This report examines recent studies on microstructural evolutions in irradiated FeCrAl alloys and point out some future studies that are needed to better understand the mechanisms of radiation damage in FeCrAl alloys and further improve their radiation tolerance. Keywords: FeCrAl alloys, high temperature oxidation, dislocation loop formation, α' phase separation, irradiation hardening Date: Monday, October 7, 2019 Time: 8:30 A.M. Place: ARMS 3115

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Recall: Seminar Notice for Tianyi Sun's Preliminary Exam. Seminar Monday, October 7, at 8:30 a.m., in ARMS 3115. Review same day, at 9:30, in ARMS 2237. Exam same day, at 10:00, in ARMS 2237
by Son, Rosemary E 23 Sep '19

23 Sep '19

Son, Rosemary E would like to recall the message, "Seminar Notice for Tianyi Sun's Preliminary Exam. Seminar Monday, October 7, at 8:30 a.m., in ARMS 3115. Review same day, at 9:30, in ARMS 2237. Exam same day, at 10:00, in ARMS 2237".

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Seminar Notice for Tianyi Sun's Preliminary Exam. Seminar Monday, October 7, at 8:30 a.m., in ARMS 3115. Review same day, at 9:30, in ARMS 2237. Exam same day, at 10:00, in ARMS 2237
by Son, Rosemary E 23 Sep '19

23 Sep '19

Dear Professors, Materials Engineering collects questions from each committee member to put together an exam packet to be presented to the student 30 minutes prior to the Prelim. Each committee member will have 15 minutes with a 5-minute follow-up after all committee members have had their questions addressed. Please see the attached form that will explain the process in more detail. I am preparing the exam packet for Tianyi Sun's Preliminary Exam. Please email me the questions for the exam by Oct. 4, the Friday before the exam at your convenience. Please email the questions only to me. I will present the questions to the exam chair, Prof. El-Azab, for review. The Schedule for the Seminar and Exam is as follows: Seminar: Monday, Oct. 7, at 8:30 a.m., in ARMS 3115 Review: Monday, Oct. 7, at 9:30, in ARMS 2237 Exam: Monday, Oct. 7, at 10:00, in ARMS 2237 Thank you, Rosemary School of Materials Engineering Purdue University Neil Armstrong Hall of Engineering 701 West Stadium Ave. Room 2200 West Lafayette, IN 47907 765-494-4105 [PU150]

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