November 2019 - Msepostdoc-list

MSE Soft Materials Summer Research Symposium
by Davis, Chelsea S 29 Jul '20

29 Jul '20

All, The 7th Annual Soft Materials Summer Research Symposium will be held this summer on Tuesday mornings at 11am in ARMS 1028. This weekly symposium will feature one or two short research talks by graduate students early in their research careers here at Purdue. All are welcome to attend. The full summer schedule is attached to this email. Please feel free to share this announcement with any colleagues or students that you think might be interested in attending. We look forward to seeing you there. Sincerely, Prof. Chelsea Davis Chelsea Davis, Ph.D.<https://polymerinterfacialmechanics.com/> Assistant Professor School of Materials Engineering Purdue University Neil Armstrong Hall of Engineering Room 2229 701 West Stadium Drive West Lafayette, IN 47907 Tel: (765) 494-9216<tel:(765)%20494-9216> Fax: (765) 494-1204<tel:(765)%20494-1204> [https://www.purdue.edu/brand/images/Purdue_University-150_Years_of_Giant_Le…] www.purdue.edu/giantleaps

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Seminar Reminder for Elizabeth Laskowski's Preliminary Exam. Monday, Dec. 2, at 11:00 a.m., in ARMS 1028 “High Temperature Dissolution Kinetics of Solids in Molten Chloride Salts”
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR “High Temperature Dissolution Kinetics of Solids in Molten Chloride Salts” By Elizabeth A. Laskowski Purdue MSE Preliminary Exam Advisor: Professor Kenneth H. Sandhage ABSTRACT Chloride based molten salts are of growing interest as heat transfer fluids and thermal energy storage media for concentrated solar power and as solvent baths for spent nuclear fuel processing and precious metal recovery. Sea-derived salts are especially attractive as they offer low cost, abundance, and nontoxic waste in addition to high temperature stability (>650C), low viscosity, and high heat capacity. As new engineering solutions seek to utilize molten chlorides, a significant barrier is finding cost-effective materials that can contain the hot fluids over extended service times due to the corrosive nature of the salts. Sparse literature deeply explores the corrosion kinetics observed for these fluids and generally kinetic assumptions are oversimplified and based purely on static corrosion tests. Literature exploring the kinetics of dissolution in molten oxides lends established models to describe the dissolution behavior observed in molten chloride studies. Understanding the kinetics of material dissolution in these salts will serve new material development to meet the demands of applications. Date: Monday, December 2, 2019 Time: 11:00 A.M. Place: ARMS 1028

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Seminar Notice for Juan Carlos Verduzco Gastelum's Preliminary Exam. Seminar, Tuesday, Dec. 10, at 10:30 a.m., in ARMS 1103. "Information Acquisition Approaches for Active Learning and its Applications to Materials Science"
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Information Acquisition Approaches for Active Learning and its Applications to Materials Science" By Juan Carlos Verduzco Gastelum Purdue MSE Preliminary Exam Advisors: Professor Esteban Marinero and Professor Alejandro Strachan ABSTRACT Development and application of machine learning models for the prediction of properties in materials science have gained momentum in the past decades. These algorithms boast the ability to make accurate, fast, and inexpensive predictions that can guide the design of experiments to the most likely candidates for success. However, predictions are entirely dependent on the amount and quality of the data used to train the fitted model. Datasets, both in experimental setups and in computational simulations for materials science, are small, and the generation of new entries remains a time consuming and expensive task. Active learning aims to inform new experiments to produce a gain in information and has been successful in reducing the number of experiments needed to discover a material with an optimized property. This work describes a new paradigm in the discovery of materials based on data science, analyzes the role of modeling in active learning applications for materials science, and benchmarks different acquisition functions in a Bayesian global optimization framework. Date: Tuesday, December 10, 2019 Time: 10:30 A.M. Place: ARMS 1028 School of Materials Engineering Purdue University Neil Armstrong Hall of Engineering 701 West Stadium Ave. Room 2200 West Lafayette, IN 47907 765-494-4105 [PU150]

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Seminar Notice for Ryan Szeto's Preliminary Exam. Seminar Tuesday, Dec. 10, at 9:30 a.m., in ARMS B071. "Investigation of Particle Properties on the Effect of Yield Stress of a Biomass Slurry"
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Investigation of Particle Properties on the Effect of Yield Stress of a Biomass Slurry" By Ryan Szeto Purdue MSE Preliminary Exam Advisors: Professor John A. Howarter and Kendra A. Erk ABSTRACT Corn stover is a lignocellulosic feedstock material that can be used for bioethanol production and alleviates problems with current first-generation biofuels. Despite the great promise of corn stover for biofuel conversion, it is hindered by its recalcitrant nature and high yield stress which is the stress necessary for flow to occur. Incorporating enzymes or dilute acid pretreatment is known to decrease the yield stress and viscosity of the system and increase pumpability. Though it is known that the value of yield stress decreases with processing, its effects on particle properties is poorly understood for corn stover particles. It is proposed that the critical parameters controlling yield stress are dependent on a maximum packing fraction that can change depending on particle shape and size distribution. The impact of aspect ratio, modulus, and roughness are explored for the effect on the value of yield stress. Characterization of these properties will give better insight and understanding of how corn stover particles are modified as a result of processing. Date: Tuesday, December 10, 2019 Time: 9:30 A.M. Place: ARMS B071 School of Materials Engineering Purdue University Neil Armstrong Hall of Engineering 701 West Stadium Ave. Room 2200 West Lafayette, IN 47907 765-494-4105 [PU150]

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Seminar Notice for Michael Park's Preliminary Exam. Seminar, Tuesday, Dec. 10, at 9:00 a.m., in ARMS 1021 "Perovskite Nickelate ReRAM for Next Generation Memory"
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Perovskite Nickelate ReRAM for Next Generation Memory" By Michael Taejoon Park Purdue MSE Preliminary Exam Advisor: Professor Shriram Ramanathan ABSTRACT The traditional semiconductor memory device scaling based on Moore's law is reaching fundamental limits. To overcome this scaling limit, alternative ways have been explored. Among potential candidates, Resistive Random-Access Memory (ReRAM) is one of great interest due to its scalability, low power consumption, and fast programming speed compared with the existing memory technology. ReRAM device uses materials including transition metal oxides that switch the resistance when an external bias is applied. This report summarizes the classification of ReRAM device based on resistive switching characteristics and the underlying mechanisms. Following that, perovskite rare-earth nickelates (RNiO3) as a promising candidate for ReRAM device are reviewed. These materials undergo distinctive metal-insulator phase transition caused by charge disproportionation when temperature decreases. In addition, electron doping through hydrogenation induces a more dramatic phase transition of the same nickelate system which give rise to resistance change by several orders of magnitude. The multi-level resistance states of hydrogen doped RNiO3 could be modulated by electric fields and it provides the potential for emerging memories. Date: Tuesday, December 10, 2019 Time: 9:00 A.M. Place: ARMS 1021

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Seminar Notice for Jose Waimin's Preliminary Exam. Seminar, Monday, Dec. 9, at 8:00 a.m., in ARMS 1021. "Impedimetric Measurement of Polymer Degradation for Non-invasive Assessment of Microbial Activity"
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Impedimetric Measurement of Polymer Degradation for Non-invasive Assessment of Microbial Activity" By Jose F. Waimin Purdue MSE Preliminary Exam Advisor: Professor Rahim Rahimi ABSTRACT As the demand for food products results in an unsustainable stress on our soils, under- standing the effects of microbial activity could pave the pathway towards more sustainable agriculture. Bacteria play essential roles in soil including decomposing materials as well as mineralizing nutrients from fertilizers into forms that crops can use. Current methods for microbial activity detection require high cost, specialized technicians, soil sampling, and lab culturing. These limitations make in-field detection hard to attain. Electrochemical sensors provide a solution for low-cost, large-scale deployment of sensors that can be easily integrated with wireless modules. This work demonstrates the feasibility of real-time microbial activity assessment by non-invasively monitoring of the biodegradation of polymers through a differential impedance method. This concept was tested by measuring the degradation of a Cellulose Acetate (CA) film in the presence of Pseudomonas aeruginosa, a decomposing microorganism commonly found in soil. The growth in microbial concentration was measured as a distinct decrease in impedance, with a sensitivity of 156 Ω/log[CFU/mL]. Further applications of this technology will include using different active materials to, not only measure degradation, but also other forms of microbial activity such as metabolic or enzymatic activity. Date: Monday, December 9, 2019 Time: 8:00 A.M. Place: ARMS 1021

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Seminar Notice for Anthony Becerril's Preliminary Exam. Seminar, Friday, Dec. 6, at 2:30, in ARMS 1109. "Destructive and Nondestructive Testing Methodologies in Concrete Durability"
by Son, Rosemary E 27 Nov '19

27 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Destructive and Nondestructive Testing Methodologies in Concrete Durability" By Anthony P. Becerril Purdue MSE Preliminary Exam Advisor: Professor Jeffrey P. Youngblood ABSTRACT Cementitious materials are one of the oldest technologies to exist and are used in most products and infrastructures such as roads, parking lots, buildings and more. Although an old technology, cementitious material production has not decreased and has had a static period of improvement in sustainability. The ongoing production rises concerns due to its environmental impact due to global warming and the thinning of the atmosphere. As of 2018, cement production is responsible for 8% of global C02 emissions. The use of sustainable, renewable materials is critical in cement research to significantly reduce the amount of carbon dioxide contributing to global warming. Compressive strength has historically has been tested to predict durability, but extensive reasons have shifted the focus more towards extensive durability testing. Some standards are considered Destructive Testing (DT) methods where tested samples are destroyed in the testing process and hence not available for further testing. DT methods are reliable in indicating durability mainly through strength testing. Additionally, there have been development of Nondestructive Testing (NDT) methods to extend usage of samples for determining durability. Although NDT preserve samples, there are arguments about the reliability of NDT over DT. Numerous DT and NDT standards evaluate cement performance through analysis of main parameters such as strength, durability, permeability, porosity and more3. Additionally, additives have been used to improve cement durability such as supplementary cementitious materials (SCM), chemical admixtures, and nanomaterials have been widely used and developed. Previous literature has shown that cellulose nanocrystals when used as an additive improves cement performance through flexural strength, microstructure enhancement, and an increase in degree of hydratioll4. With the increased demand for more sustainable cement production, cellulose as an additive for cement provides a resource that is renewable, biodegradable, while also improving environmental, economic, and health impacts. In this work, concrete durability testing with DT and NDT methods will be compared to address challenges, such as reliability, in concrete research and industry practices. Additionally, cellulose nanocrystals as an additive in cement production will be reviewed. Lastly, current research on cement paste durability advancement with nano-additives will be addressed. Date: Friday, December 6, 2019 Time: 2:30 P.M. Place: ARMS 1109

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Seminar Notice for Elizabeth Laskowski's Preliminary Exam. Monday, Dec. 2, at 11:00 a.m., in ARMS 1028 “High Temperature Dissolution Kinetics of Solids in Molten Chloride Salts”
by Son, Rosemary E 26 Nov '19

26 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR “High Temperature Dissolution Kinetics of Solids in Molten Chloride Salts” By Elizabeth A. Laskowski Purdue MSE Preliminary Exam Advisor: Professor Kenneth H. Sandhage ABSTRACT Chloride based molten salts are of growing interest as heat transfer fluids and thermal energy storage media for concentrated solar power and as solvent baths for spent nuclear fuel processing and precious metal recovery. Sea-derived salts are especially attractive as they offer low cost, abundance, and nontoxic waste in addition to high temperature stability (>650C), low viscosity, and high heat capacity. As new engineering solutions seek to utilize molten chlorides, a significant barrier is finding cost-effective materials that can contain the hot fluids over extended service times due to the corrosive nature of the salts. Sparse literature deeply explores the corrosion kinetics observed for these fluids and generally kinetic assumptions are oversimplified and based purely on static corrosion tests. Literature exploring the kinetics of dissolution in molten oxides lends established models to describe the dissolution behavior observed in molten chloride studies. Understanding the kinetics of material dissolution in these salts will serve new material development to meet the demands of applications. Date: Monday, December 2, 2019 Time: 11:00 A.M. Place: ARMS 1028

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Seminar Reminder for Ziyun Huang's Preliminary Exam, Wednesday, Nov. 27, at 1:00, in ARMS 1021 " Thermodynamically-driven Massive Spalling in Solder Joints"
by Son, Rosemary E 26 Nov '19

26 Nov '19

Please consider attending the following: MATERIALS ENGINEERING SEMINAR "Thermodynamically-driven Massive Spalling in Solder Joints" By Ziyun Huang Purdue MSE Preliminary Exam Advisors: Professor Carol A. Handwerker and Professor John E. Blendell ABSTRACT Solder joint plays an important role in present packaging industry and has a great impact on overall reliability property of chips. This review will mainly focus on massive spalling phenomenon in solders and its thermodynamic driving force. The necessary condition for spalling to happen is that at least one of the active components has limited amount, and local equilibrium changes as the reactive constituent is consumed. Specifically, massive spalling results from two mechanism (1) grain boundary penetration and (2) microvoids aggregation. Both high-lead and lead-free solders will be considered due to environmental concern of lead. For each case, industrial methods to inhibit massive spalling have been discussed. However, increased interfacial energy as a consequence of spalling has never been directly proved, and more experiments are needed to further understand this problem. Date: Wednesday, November 27, 2019 Time: 1:00 P.M. Place: ARMS 1021

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MSE Safety & Equipment Newsletter for November/December 2019
by Erk, Kendra A 25 Nov '19

25 Nov '19

PDF of newsletter available here: https://engineering.purdue.edu/Intranet/Groups/Schools/MSE/Facilities/Safet… MSE Safety & Equipment Newsletter for November/December 2019 **** Important Upcoming Dates **** · Purdue Winter Recess, Dec. 23 through Jan. 1. Exercise caution when working in the lab during the recess as few (if any) personnel will be on campus to provide assistance. **** MSE Lab Safety Blackboard Course Updates **** · Guidance and links for Accident & Near-Miss reporting Reminder: To self-enroll in this Blackboard course, click here<https://mycourses.purdue.edu/webapps/blackboard/execute/viewCatalog?id=&typ…> . **** Annual Safety Training Reminder **** As described in the MSE safety training policy (posted here<https://engineering.purdue.edu/Intranet/Groups/Schools/MSE/Facilities/Safet…>), each academic year, all undergraduate students, graduate students, and postdoctoral researchers are required to complete the MSE-specific safety training (slides & quiz) administered through Blackboard. A list of researchers who have/have not completed the training will be provided to Prof. Bahr and MSE faculty members at the end of the semester. **** PPE Reminder **** Physical and health hazards and the required PPE for each MSE lab space are posted on the lab’s main door. Required PPE typically includes impact-resistant safety glasses, long pants, closed-toed shoes, and, for CHP labs, a lab coat. To encourage PPE use, a “three-strike” infraction policy has been adopted, described below. For example, an infraction could be not wearing safety glasses in a lab space where safety glasses are required. · First infraction: warning email with supervisor copied · Second infraction: lab access temporarily suspended · Third infraction: lab access permanently suspended **** XRD Lab Clean-Up **** Prof. Blendell and the Equipment Committee will be removing two old XRDs and other related equipment in the XRD lab (ARMS 2093). During this process, Prof. Blendell will label equipment, components, and other things as “to-go” by Monday, Dec 2nd. These items will then be sent to surplus or thrown away. Contact Prof. Blendell<mailto:blendell@purdue.edu> to inquire about specific items. **** Mechanical Testing Equipment Update**** If you wish to use any of the following equipment, please make sure you receive training from Jenni Fifer<mailto:fiferj@purdue.edu> if you are not already trained; and please schedule your time with the equipment using the following Google Calendars: · Charpy Impact Test<https://calendar.google.com/calendar?cid=NzJ2YW9nMHJlNGljamtsdWo4bGNpN3U2cj…> (ARMS 2191) · ADMET Load Frame 1<https://calendar.google.com/calendar?cid=NDAya2ZzbHVsbW5qa3VjbmpsZWk0OHIzZ3…> (ARMS 2191) and ADMET Load Frame 2<https://calendar.google.com/calendar?cid=cnBmZWRjaTBlM2dzY2E2cGY0MmtzNGQzb2…> (ARMS 2191) · Sintech Load Frame<https://calendar.google.com/calendar/b/1?cid=djBuN3Q3cjd2djhtbHI4NXJsbmFnbj…> (ARMS B146) · Vickers Microhardness<https://calendar.google.com/calendar/b/1?cid=cGFpZ2VzMTQ5OUBnbWFpbC5jb20> (ARMS 2130) · MTS Load Frame<https://calendar.google.com/calendar/r/settings/calendar/aGNzY21lZGRxNHAwdD…> (ARMS B146) - must be trained before accessing this calendar. **** Equipment Reporting Reminder **** If you encounter a piece of broken equipment, or have any questions about a specific piece of equipment, you should contact a member of the MSE Technical Staff: · For general equipment (and associated checklists): Tim VanMeter<mailto:tcvanmet@purdue.edu>, Darren Pauly<mailto:dpauly@purdue.edu> · For mechanical testing equipment: Jenni Fifer<mailto:fiferj@purdue.edu> · For analytical (iLab) equipment: Talukder Alam<mailto:alam18@purdue.edu> **** Important Links and Contact Information **** · For general safety questions, concerns, and lab access issues: mse-safety(a)purdue.edu<mailto:mse-safety@purdue.edu> or speak directly to MSE Safety Officer Jenni Fifer<mailto:fiferj@purdue.edu> (ARMS 2207) · For iLab equipment training and issues: Talukder Alam<mailto:alam18@purdue.edu> (ARMS 2207) · Equipment/Safety/Consumables Reporting Form<https://purdue.ca1.qualtrics.com/jfe/form/SV_7QcGyO9IVMwWRPD?_ga=2.24554381…> · Purdue REM Researcher’s Guide<https://www.purdue.edu/ehps/rem/laboratory/researchers.html#cs2> (all new researchers should check this out...) · ARMS general safety information<https://engineering.purdue.edu/Intranet/Groups/Facilities/ArmstrongHall> Thanks for reading everyone and have a GREAT holiday season!   Prof. Erk and the MSE Safety Committee 

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